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B.H. Lee 2 Articles
Fabrication of Fe-TiC Composite by High-Energy Milling and Spark-Plasma Sintering
N.Q. Tuan, H.X. Khoa, N.H. Vieta, Y.H. Lee, B.H. Lee, J.S. Kim
J Powder Mater. 2013;20(5):338-344.
DOI: https://doi.org/10.4150/KPMI.2013.20.5.338
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AbstractAbstract PDF
Fe-TiC composite was fabricated from Fe and TiC powders by high-energy milling and subsequent spark-plasma sintering. The microstructure, particle size and phase of Fe-TiC composite powders were investigated by field emission scanning electron microscopy and X-ray diffraction to evaluate the effect of milling conditions on the size and distribution of TiC particles in Fe matrix. TiC particle size decreased with milling time. The average TiC particle size of 38 nm was obtained after 60 minutes of milling at 1000 rpm. Prepared Fe-TiC powder mixture was densified by spark-plasma sintering. Sintered Fe-TiC compacts showed a relative density of 91.7~96.2%. The average TiC particle size of 150 nm was observed from the FE-SEM image. The microstructure, densification behavior, Vickers hardness, and fracture toughness of Fe-TiC sintered compact were investigated.

Citations

Citations to this article as recorded by  
  • Synthesis of Cu-based TiCx composites via in-situ reaction between CuxTi melt and dissolvable solid carbon
    Lei Guo, Yang Yang, Xiaochun Wen, Han Gao, Zhe Wang, Zhancheng Guo
    Powder Technology.2020; 362: 375.     CrossRef
  • Microstructure and Electrical Property of Ex-Situ and In-Situ Copper Titanium Carbide Nanocomposites
    Nguyen Hoang Viet, Nguyen Thi Hoang Oanh
    Metals.2020; 10(6): 735.     CrossRef
  • Kinetic Models for the in Situ Reaction between Cu-Ti Melt and Graphite
    Lei Guo, Xiaochun Wen, Zhancheng Guo
    Metals.2020; 10(2): 267.     CrossRef
  • Fabrication of core‐shell structured TiC–Fe composite powders by fluidized bed chemical vapor deposition
    Cheng Liu, Yafeng Yang, Pengpeng Lv, Junjie Guo, Maoqiao Xiang, Qingshan Zhu
    Journal of the American Ceramic Society.2019; 102(8): 4470.     CrossRef
  • Effect of mechanical alloying on the synthesis of Fe-TiC nanocomposite
    Ali Reza Jam, Mansour Razavi, Leila Nikzad
    Science and Engineering of Composite Materials.2017; 24(5): 739.     CrossRef
  • Synthesis and analysis of nanocrystalline β1-Cu3Al and β2-NiAl intermetallic-reinforced aluminum matrix composite by high energy ball milling
    Hong-Hai Nguyen, Minh-Thuyet Nguyen, Won Joo Kim, Jin-Chun Kim
    Metals and Materials International.2017; 23(1): 202.     CrossRef
Fabrication of Fe-TiB2 Composite Powder by High-Energy Milling and Subsequent Reaction Synthesis
H.X. Khoa, N.Q. Tuan, Y.H. Lee, B.H. Lee, N.H. Viet, J.S. Kim
J Powder Mater. 2013;20(3):221-227.
DOI: https://doi.org/10.4150/KPMI.2013.20.3.221
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  • 9 Citations
AbstractAbstract PDF
TiB_2-reinforced iron matrix composite (Fe-TiB_2) powder was in-situ fabricated from titanium hydride (TiH_2) and iron boride (FeB) powders by the mechanical activation and a subsequent reaction. Phase formation of the composite powder was identified by X-ray diffraction (XRD). The morphology and phase composition were observed and measured by field emission-scanning electron microscopy (FE-SEM) and energy-dispersive X-ray spectroscopy (EDS), respectively. The results showed that TiB_2 particles formed in nanoscale were uniformly distributed in Fe matrix. Fe_2B phase existed due to an incomplete reaction of Ti and FeB. Effect of milling process and synthesis temperature on the formation of composite were discussed.

Citations

Citations to this article as recorded by  
  • Low temperature controllable synthesis of transition metal and rare earth borides mediated by molten salt
    Xueyin Liu, Quanli Jia, Shaowei Zhang, William E. Lee
    International Materials Reviews.2024; 69(2): 107.     CrossRef
  • In Situ Spark Plasma Sintering, Microstructure and Mechanical Properties of Fe-15Cr-2Mn-1.5Al Matrix Composites Reinforced with TiB2 and CrFeB
    Jian Liu, Min Wu, Bin Wang, Wei Xu, Weiping Chen, Fangfang Liu
    JOM.2023; 75(3): 886.     CrossRef
  • Glass-Forming Ability and Magnetic Properties of Al82Fe16Ce2 and Al82Fe14Mn2Ce2 Alloys Prepared by Mechanical Alloying
    Nguyen Hong Hai, Nguyen Hoang Viet, Nguyen Thi Hoang Oanh
    Applied Sciences.2023; 14(1): 152.     CrossRef
  • Powder metallurgy processed TiB2-reinforced steel matrix composites: a review
    Silani Sahoo, Bharat Bhushan Jha, Animesh Mandal
    Materials Science and Technology.2021; 37(14): 1153.     CrossRef
  • Synthesis of Cu-based TiCx composites via in-situ reaction between CuxTi melt and dissolvable solid carbon
    Lei Guo, Yang Yang, Xiaochun Wen, Han Gao, Zhe Wang, Zhancheng Guo
    Powder Technology.2020; 362: 375.     CrossRef
  • Microstructure and Electrical Property of Ex-Situ and In-Situ Copper Titanium Carbide Nanocomposites
    Nguyen Hoang Viet, Nguyen Thi Hoang Oanh
    Metals.2020; 10(6): 735.     CrossRef
  • Mechanical and Wear Behaviour of Hot-Pressed 304 stainless Steel Matrix Composites Containing TiB2 Particles
    Silani Sahoo, Bharat B. Jha, Tarasankar Mahata, Jyothi Sharma, Tammana S. R. Ch. Murthy, Animesh Mandal
    Transactions of the Indian Institute of Metals.2019; 72(5): 1153.     CrossRef
  • Effect of volume fraction of reinforcement phase on mechanical behavior of ultra-high-temperature composite consisting of iron matrix and TiB2 particulates
    Babak Jahani, Mehdi Salimi Jazi, Fardad Azarmi, Andrew Croll
    Journal of Composite Materials.2018; 52(5): 609.     CrossRef
  • Impression creep behaviour of TiB2 particles reinforced steel matrix composites
    S. Sahoo, B. B. Jha, T.S. Mahata, J. Sharma, T. S. R. Ch. Murthy, A. Mandal
    Materials Science and Technology.2018; 34(16): 1965.     CrossRef

Journal of Powder Materials : Journal of Powder Materials